北检（北京）检测技术研究院

1.1 This test method covers the determination of carbonate content of soils and soft rock which can be readily broken down by mechanical effort. It is a gasometric method that utilizes a simple portable apparatus. Results should be clearly stated as the calcite equivalent in percent because different carbonate species cover a wide range of percent calcite equivalent as shown below for a number of carbonates:

For example， a 100 % dolomite would be expected to yield 108.6 % calcite equivalent while 100 % siderite would yield only 86.4 % calcite equivalent. Calcite and aragonite reactions will typically complete within about 10 min. This method does not distinguish between the carbonate species and such determination must be made using quantitative chemical analysis methods such as atomic absorption.

1.2 The values stated in SI units are to be regarded as the standard.

1.3 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D 6026.

1.4 The method used to specify how data are collected， calculated， or recorded in this standard is not directly related to the accuracy to which the data can be applied in design or other uses， or both. How one applies the results obtained using this standard is beyond its scope.

1.5 This standard does not purport to address all of the safety concerns， if any， associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific precaution statements， see Section 8.

The water content of soil is used throughout geotechnical engineering practice， both in the laboratory and in the field. Results are sometimes needed within a short time period and in locations where it is not practical to install an oven or to transport samples to an oven. This test method is used for these occasions.

The results of this test have been used for field control of compacted embankments or other earth structures such as in the determination of water content for control of soil moisture and dry density within a specified range.

This test method requires specimens consisting of soil having all particles smaller than the No. 4 sieve size.

This test method may not be as accurate as other accepted methods such as Test Method D 2216. Inaccuracies may result because specimens are too small to properly represent the total soil， from clumps of soil not breaking up to expose all the available water to the reagent and from other inherent procedural， equipment or process inaccuracies. Therefore， other methods may be more appropriate when highly accurate results are required， or when the use of test results is sensitive to minor variations in the values obtained.

Note 18212;The quality of the result produced by this standard is dependent on the competence of the personnel performing it， and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D 3740 are generally considered capable of competent and objective testing/sampling/inspection. Users of this standard are cautioned that compliance with Practice D 3740 does not in itself ensure reliable results. Reliable results depend on many factors; Practice D 3740 provides a means of evaluating some of those factors.

1.1 This test method outlines procedures for determining the water (moisture) content of soil by chemical reaction using calcium carbide as a reagent to react with the available water in the soil producing a gas. A measurement is made of the gas pressure produced when a specified mass of wet or moist soil is placed in a testing device with an appropriate volume of reagent and mixed.

1.2 This test method is not intended as a replacement for Test Method D 2216; but as a supplement when rapid results are required， when testing is done in field locations， or where an oven is not practical for use. Test Method D 2216 is to be used as the test method to compare for accuracy checks and correction.

1.3 This test method is applicable for most soils. Calcium carbide， used as a reagent， reacts with water as it is mixed with the soil by shaking and agitating with the aid of steel balls in the apparatus. To produce accurate results， the reagent must react with all the water which is not chemically hydrated with soil minerals or compounds in the soil. Some highly plastic clay soils or other soils not friable enough to break up may not produce representative results because some of the water may be trapped inside soil clods or clumps which cannot come in contact with the reagent. There may be some soils containing certain compounds or chemicals that will react unpredictably with the reagent and give erroneous results. Any such problem will become evident as calibration or check tests with Test Method D 2216 are made. Some soils containing compounds or minerals that dehydrate with heat (such as gypsum) which are to have special temperature control with Test Method D 2216 may not be affected (dehydrated) in this test method.

1.4 This test method is limited to using calcium carbide moisture test equipment made for 20 g， or larger， soil specimens and to testing soil which contains particles no larger than the No. 4 Standard sieve size.

This standard does not purport to addres......